3,4,5,6-四氢-2-嘧啶硫醇合成路线 (共 24 条)
反应条件
sodium tetrahydroborate in acetonitrile T=20°C; Reduction; 7 h;
参考文献
Shutalev
Chemistry of Heterocyclic Compounds, 1998 , vol. 34, # 2 p. 204 - 206
参考文献
Bogatskii, A.V.; Luk'yanenko, N. G.; Kirichenko, T. I.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1124 - 1129
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 6 p. 1301 - 1307
反应条件
sodium tetrahydroborate; trifluoroacetic acid in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Shutalev, A. D.; Komarova, E. N.; Ignatova, L. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993 , vol. 29, # 10 p. 1182 - 1191
Khimiya Geterotsiklicheskikh Soedinenii, 1993 , # 10 p. 1378 - 1388
反应条件
hydrogen sulfide in ethanol 1.5 h; Heating;
参考文献
Synthesis, , # 11 p. 908 - 910
反应条件
triethanolamine; triethylamine in N,N-dimethyl-formamide 45 h; Heating;
参考文献
Ramadas, K.; Janarthanan, N.
Journal of Chemical Research, Miniprint, 1998 , # 5 p. 1101 - 1108
反应条件
in butan-1-ol 0.166667 h; Heating;
参考文献
Kibbel, H. U.; Kuecken, M.; Peters, E.; Weber, H.
Journal fuer Praktische Chemie (Leipzig), 1981 , vol. 323, # 1 p. 41 - 48
参考文献
Journal of the American Chemical Society, , vol. 78, p. 1618
反应条件
tetraphosphorus decasulfide; xylene
参考文献
Justus Liebigs Annalen der Chemie, , vol. 607, p. 67,76
反应条件
in acetonitrile 0.5 h; Heating;
参考文献
Synthetic Communications, , vol. 25, # 21 p. 3381 - 3387
反应条件
in acetonitrile 0.2 h; Heating;
参考文献
Synthetic Communications, , vol. 25, # 21 p. 3381 - 3387