in neat (no solvent) from As mirror with CH3 radical (thermal decompn. of tetramethyl lead at low pressure in H2 stream);; pptn. on cooling with liquid air; fractionated distn.;;
参考文献
Paneth, F.
Transactions of the Faraday Society, 1934 , vol. 30, p. 179
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Gmelin Handbook: As: MVol., 52, page 184 - 186
Steinkopf; Dudek
Chemische Berichte, 1928 , vol. 61, p. 1910
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Valeur; Gailliot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1927 , vol. 185, p. 958