环丙烷-1,2-二羧酸二乙酯合成路线 （共 11 条）
反应条件
in hexane; ethyl acetate; toluene
参考文献
E. I. Du Pont de Nemours and Company; Degussa Aktiengesellschaft
Patent: US5700761 A1, 1997 ;
反应条件
palladium diacetate in benzene T=40°C;
参考文献
Majchrzak, Michal W.; Kotelko, Antoni; Lambert, Joseph B.
Synthesis, 1983 , # 6 p. 469 - 470
反应条件
copper(II) bis(trifluoromethanesulfonate); lithium diisopropyl amide in tetrahydrofuran T=-78°C; 30 h;
参考文献
Kobayashi, Yoshiro; Taguchi, Takeo; Morikawa, Tsutomu; Tokuno, Etsuko; Sekiguchi, Shoh
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 1 p. 262 - 267
反应条件
N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate in N,N-dimethyl-formamide 24 h; Ambient temperature;
参考文献
Chaoguo, Yan; Qiangzhi, Kong; Wenxing, Lu; Jitao, Wu
Synthetic Communications, 1992 , vol. 22, # 12 p. 1651 - 1653
反应条件
in toluene; mineral oil; tert-butyl alcohol
参考文献
Merck and Co., Inc.
Patent: US4617304 A1, 1986 ;
反应条件
in water; toluene; mineral oil
参考文献
MERCK and CO. INC.
Patent: EP159264 B1, 1991 ;
反应条件
molybdenum hexacarbonyl T=65°C; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Doyle, Michael P.; Davidson, James G.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1538 - 1539
反应条件
sodium hydroxide in water
参考文献
E. I. Du Pont de Nemours and Company; Degussa Aktiengesellschaft
Patent: US5700761 A1, 1997 ;
反应条件
1: methanol / Heating 2: diethyl ether View Scheme
参考文献
Mohr, Peter; Waespe-Sarcevic, Nada; Tamm, Christoph; Gawronska, Krystyna; Gawronsky, Jacek K.
Helvetica Chimica Acta, 1983 , vol. 66, # 8 p. 2501 - 2511
反应条件
sodium hydroxide; acetic anhydride 1.) 15 h, reflux, 2.) 0.5 h, reflux; Multistep reaction;
参考文献
Synthesis, , # 6 p. 469 - 470
