1-(3-丁烯-1-基)-4-甲氧基苯合成路线 (共 30 条)
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 3 h; Heating;
参考文献
Kanehara, Masayuki; Oumi, Yasunori; Sano, Tsuneji; Teranishi, Toshiharu
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 8 p. 1589 - 1597
反应条件
[VO(OEt)Cl2] in dichloromethane -75 deg C, 2 h; RT, 4 h;
参考文献
Hirao, Toshikazu; Fujii, Takashi; Ohshiro, Yoshiki
Tetrahedron Letters, 1994 , vol. 35, # 43 p. 8005 - 8008
反应条件
in diethyl ether Condensation; 16 h; Heating;
参考文献
Newcomb; Choi; Toy
Canadian Journal of Chemistry, 1999 , vol. 77, # 5-6 p. 1123 - 1135
反应条件
1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere 1.2: 0 - 20 °C / Inert atmosphere 2.1: InOTf / toluene / 14 h / -20 - 20 °C / Inert atmosphere View Scheme
参考文献
Chemical Communications, , vol. 47, # 2 p. 692 - 694
反应条件
1: base 3: collidinium trifulorosulfonate / toluene / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 7 p. 1305 - 1308
反应条件
iron(III) chloride; potassium carbonate in tetrahydrofuran; diethyl ether T=10 - 15°C; 18 h;
参考文献
Zubritskii, L. M.; Romashchenkova, N. D.; Petrov, A. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2157 - 2167
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2465 - 2477
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride Addition; demetallation, aromatization; 8 h; Heating;
参考文献
Wei, Li Lan; Lai, Ming Chih; Ong, Chi Wi
Tetrahedron Letters, 2000 , vol. 41, # 18 p. 3407 - 3410
反应条件
1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C / |Inert atmosphere 2: triphenylphosphine; 1H-imidazole; bromine / dichloromethane / 17 h / 20 °C / |Inert atmosphere 3: potassium carbonate / acetone / 38 h / |Reflux; |Inert atmosphere 4: (NH4)6[Mo7O24]*4H2O; dihydrogen peroxide / methanol; water / 2.5 h / 0 - 20 °C / |Inert atmosphere 5: N,N,N',N,-tetramethylethylenediamine; iron (III) acetylacetonate; CPME / 18 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 24 p. 12593 - 12628
反应条件
1: potassium carbonate / acetone / 38 h / |Reflux; |Inert atmosphere 2: (NH4)6[Mo7O24]*4H2O; dihydrogen peroxide / methanol; water / 2.5 h / 0 - 20 °C / |Inert atmosphere 3: N,N,N',N,-tetramethylethylenediamine; iron (III) acetylacetonate; CPME / 18 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 24 p. 12593 - 12628
反应条件
1: (NH4)6[Mo7O24]*4H2O; dihydrogen peroxide / methanol; water / 2.5 h / 0 - 20 °C / |Inert atmosphere 2: N,N,N',N,-tetramethylethylenediamine; iron (III) acetylacetonate; CPME / 18 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 24 p. 12593 - 12628