反应条件
in neat (no solvent) byproducts: NaCl; under Ar, 1 equiv. of CaCl2 and 1 equiv. of Na2CN2, grinding in an agatemortar, welding into a Ta container, sealing into an evacuated silica t ube, heating up to 1200 K in 12 h, 3 d; furnace was switched off, cooling to room temp.;
参考文献
Reckeweg, Olaf; DiSalvo, Francis J.
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2008 , vol. 63, # 5 p. 530 - 536
