4'-甲氧基-3-(4-甲氧基苯基)苯丙酮合成路线 （共 15 条）
反应条件
magnesium; zinc(II) chloride 0.416667 h;
参考文献
Saikia, Anil; Barthakur, Madan Gopal; Boruah, Romesh Chandra
Synlett, 2005 , # 3 art. no. D32504ST, p. 523 - 525
反应条件
acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II); potassium carbonate; butan-1-ol 1.5 h; Reflux; chemoselective reaction;
参考文献
Ding, Boqiang; Zhang, Zhenfeng; Liu, Yangang; Sugiya, Masashi; Imamoto, Tsuneo; Zhang, Wanbin
Organic Letters, 2013 , vol. 15, # 14 p. 3690 - 3693
反应条件
C15H17N2Ru(1+)*F6P(1-); sodium t-butanolate in toluene T=110°C; 17 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 53, # 12 p. 1450 - 1455
反应条件
potassium carbonate 0.075 h; Microwave irradiationSonicationReflux;
参考文献
Tetrahedron Letters, , vol. 53, # 9 p. 1160 - 1162
反应条件
potassium hydroxide in toluene T=110°C; 24 h; Sealed tubeSchlenk techniqueInert atmosphere; TemperatureTime;
参考文献
Xu, Qing; Chen, Jianhui; Tian, Haiwen; Yuan, Xueqin; Li, Shuangyan; Zhou, Chongkuan; Liu, Jianping
Angewandte Chemie - International Edition, 2014 , vol. 53, # 1 p. 225 - 229
Angew. Chem., 2014 , vol. 126, # 1 p. 229 - 233,5
反应条件
sodium tetrahydroborate; nickel dichloride in methanol T=20°C; 0.166667 h;
参考文献
Khurana, Jitender M.; Kandpal, Bhaskar M.; Kukreja, Gagan; Sharma, Purnima
Canadian Journal of Chemistry, 2006 , vol. 84, # 8 p. 1019 - 1023
反应条件
trifluoromethanesulfonic acid anhydride in 1,2-dichloro-ethane 3 h; Heating;
参考文献
Nenajdenko, Valentine G.; Baraznenok, Ivan L.; Balenkova, Elizabeth S.
Tetrahedron Letters, 1996 , vol. 37, # 24 p. 4199 - 4202
反应条件
pyrrolidine in N,N-dimethyl-formamide T=115°C; 6 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 20 p. 5456 - 5459
反应条件
1: N,N-dicyclohexylmethylamine; potassium carbonate; bis(dibenzylideneacetone)-palladium(0); cataCXium PIntB / N,N-dimethyl-formamide / 0.5 h / 100 °C / Molecular sieve; Inert atmosphere 2: pyrrolidine / N,N-dimethyl-formamide / 6 h / 115 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 13, # 20 p. 5456 - 5459
反应条件
1: sodium hydroxide / ethanol / 4 h / 0 - 20 °C 2: acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II); butan-1-ol; potassium carbonate / 1.5 h / |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 14 p. 3690 - 3693
