全氟(2-甲基-3-氧杂己基)氟化物合成路线 (共 39 条)
反应条件
potassium fluoride T=70°C; Product distribution / selectivity;
参考文献
ASAHI GLASS COMPANY LTD.
Patent: EP1352892 A1, 2003 ;
Location in patent: Page/Page column 14 ;
反应条件
bis(diethylamino)methane in acetonitrile T=-15°C;
参考文献
Igumnov; Lekontseva; Shipigusev; Mukhametshin
Russian Journal of Applied Chemistry, 2005 , vol. 78, # 3 p. 435 - 437
反应条件
triethylammoniumperfluorocyclobutane tetrafluoroborate in acetonitrile 2 h;
参考文献
Pasenok, Sergej V.; De Roos, Marijn E.; Appel, Wolfgang K.
Tetrahedron, 1996 , vol. 52, # 29 p. 9755 - 9758
反应条件
hexafluorocyclopropylene oxide; cesium fluoride in diethylene glycol dimethyl ether T=20°C; 1 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, # 2 p. 311 - 315
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 2 p. 392 - 395
参考文献
EP1548014 A1, ;
Page/Page column 15 ;
反应条件
potassium fluoride T=80 - 90°C; 4 h;
参考文献
EP1574497 A1, ;
Page/Page column 19 ;
反应条件
N,N,N',N'-tetramethyl-urea in diethylene glycol dimethyl ether 3 h; Ambient temperature;
参考文献
Kawa, Hajimu; Yamaguchi, Fumihiko; Ishikawa, Nobuo
Journal of Fluorine Chemistry, 1982 , vol. 20, p. 475 - 486
反应条件
1: 2,3,3,3-tetrafluoro-2-(pentafluorophenoxy)propionyl fluoride With potassium fluoride in 1.4-dicyano 1-butene; bis [2-(2-methoxyethoxy)ethyl] ether 0.5 h; 2: hexafluorocyclopropylene oxide in 1.4-dicyano 1-butene; bis [2-(2-methoxyethoxy)ethyl] ether T=25 - 29°C; Product distribution / selectivity;
参考文献
EP939752 B1, ;
Page/Page column 5-6 ;
反应条件
cesium fluoride in diethylene glycol dimethyl ether 2 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, # 2 p. 311 - 315
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 2 p. 392 - 395
反应条件
potassium fluoride in diethylene glycol dimethyl ether
参考文献
Russian Journal of Applied Chemistry, , vol. 86, # 3 p. 376 - 386
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), , vol. 86, # 3 p. 376 - 386,10