全氟(2-甲基-3-氧杂己基)氟化物合成路线 (共 39 条)
反应条件
carbon dioxide in various solvent(s) T=30°C; KineticsActivation energy; Further Variations:SolventsTemperaturessolvent viscosity;
参考文献
Journal of the American Chemical Society, , vol. 123, # 30 p. 7199 - 7206
反应条件
activated carbon BAU in neat (no solvent) T=130°C; Reagent/catalystTemperature;
参考文献
Russian Journal of Applied Chemistry, , vol. 86, # 8 p. 1243 - 1251
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), , vol. 86, # 8 p. 1269 - 1277,9
反应条件
potassium fluoride in diethylene glycol dimethyl ether 24 h; Ambient temperature; Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 25, p. 241 - 254
反应条件
1: With 1,2,2-trifluoro-trichloroethane; fluorine 2: With NAF T=140°C; 10 h; Title compound not separated from byproducts;
参考文献
Okazoe, Takashi; Murotani, Eisuke; Watanabe, Kunio; Itoh, Masahiro; Shirakawa, Daisuke; Kawahara, Kengo; Kaneko, Isamu; Tatematsu, Shin
Journal of Fluorine Chemistry, 2004 , vol. 125, # 11 SPEC. ISS. p. 1695 - 1701
反应条件
potassium fluoride; ethyl fluorooxolate in diethylene glycol dimethyl ether 14 h; Heating; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 80, # 2 p. 125 - 134
反应条件
Cu2Cl2 in acetonitrile oligomerization; Title compound not separated from byproducts;
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 12 p. 1715 - 1720
反应条件
T=20°C; 24 h; Yield given;
参考文献
Russian Journal of Organic Chemistry, , vol. 33, # 3 p. 300 - 302
Zhurnal Organicheskoi Khimii, , vol. 33, # 3 p. 344 - 347
反应条件
in tetrahydrofuran T=30°C; other solvents, other temperatures (0-40 deg C), δH(excit.), rate constants of chain growth and chain transfer; Rate constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, p. 444 - 448
Zhurnal Organicheskoi Khimii, , vol. 20, # 3 p. 493 - 498
反应条件
potassium fluoride T=80 - 90°C; 4 h; Pyrolysis; Product distribution / selectivity;
参考文献
WO2005/123650 A1, ;
Page/Page column 15 ;
反应条件
N,N-dimethyl-formamide T=130°C; Yield given;
参考文献
Ohsaka, Yohnosuke; Amimoto, Yoshio; Takaki, Shoji
Journal of Fluorine Chemistry, 1982 , vol. 21, p. 54