全氟(2-甲基-3-氧杂己基)氟化物合成路线 （共 39 条）
反应条件
sodium carbonate in diethylene glycol dimethyl ether T=115 - 130°C; other solvent; KineticsRate constantThermodynamic data;
参考文献
Yuminov, V. S.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 8 p. 1037 - 1039
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 8 p. 1142 - 1144
反应条件
T=-5 - 150°C; P=750.075 Torr; Heating / reflux;
参考文献
Asahi Glass Company, Limited
Patent: EP1679298 A1, 2006 ;
Location in patent: Page/Page column 10 ;
反应条件
T=20°C; Recombination; Decarbonylation; 8 h; Irradiation;
参考文献
Tonelli, Claudio; Tortelli, Vito
Journal of Fluorine Chemistry, 2000 , vol. 101, # 1 p. 117 - 123
反应条件
in tetrahydrofuran 0°C, 2 h , ratio of products = 1:1;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 2.2, page 20 - 27
反应条件
in tetrahydrofuran ratio of C6F5C(O)CF(CF3)OC3F7 and 4-C6F5-C6F4C(O)CF(CF3)OC3F7 = 41:55 after 4 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 2.2, page 20 - 27
反应条件
triethylamine T=5 - 20°C;
参考文献
Studnev, Yu. N.; Kinosh, O. F.; Zabornya, V. V.; Frolovskii, V. A.; Stolyarov, V. P.; Rozantsev, G. G.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.1 p. 1162 - 1163
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1292 - 1293
反应条件
lithium iodide T=180°C; 6.5 h;
参考文献
Fukaya, Haruhiko; Hayashi, Eiji; Hayakawa, Yoshio; Abe, Takashi
Journal of Fluorine Chemistry, 1997 , vol. 83, # 2 p. 117 - 123
反应条件
T=-5 - 150°C; P=750.075 Torr; Heating / reflux;
参考文献
Asahi Glass Company, Limited
Patent: EP1679298 A1, 2006 ;
Location in patent: Page/Page column 10 ;
参考文献
Fenichev; Babenko; Bispen; Moldavskii
Russian Journal of Applied Chemistry, 2013 , vol. 86, # 3 p. 376 - 386
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), 2013 , vol. 86, # 3 p. 376 - 386,10
反应条件
in diethyl ether -20°C, 12 d;
参考文献
Journal of Fluorine Chemistry, , vol. 13, p. 337,339, 340, 344, 348
