全氟(2-甲基-3-氧杂己基)氟化物合成路线 （共 39 条）
反应条件
sodium carbonate pyrolysis;
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 1409 - 1412
Zhurnal Organicheskoi Khimii, , vol. 17, # 8 p. 1587 - 1590
反应条件
sodium carbonate T=270°C; 1.8 h; Product distribution / selectivity;
参考文献
EP1352892 A1, ;
Page/Page column 15 ;
反应条件
1: With sodium hydroxide in methanol 2: T=380°C; Pyrolysis;
参考文献
WO2005/121118 A1, ;
Page/Page column 20-21 ;
反应条件
sodium carbonate pyrolysis;
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 1409 - 1412
Zhurnal Organicheskoi Khimii, , vol. 17, # 8 p. 1587 - 1590
反应条件
sodium carbonate in diethylene glycol dimethyl ether T=115 - 130°C; other solvent; KineticsRate constantThermodynamic data;
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 8 p. 1037 - 1039
Zhurnal Organicheskoi Khimii, , vol. 31, # 8 p. 1142 - 1144
反应条件
in diethyl ether -20°C, 12 d;
参考文献
Journal of Fluorine Chemistry, , vol. 13, p. 337,339, 340, 344, 348
反应条件
sodium carbonate in diethylene glycol dimethyl ether
T=140 - 150°C; 2 h;
参考文献
Lebedev; Berenblit; Starobin; Gubanov
Russian Journal of Applied Chemistry, 2005 , vol. 78, # 10 p. 1640 - 1645
反应条件
1: 75 percent Spectr. / benzonitrile
2: 49 percent / 50percent aq. NaOH / benzonitrile
View Scheme
参考文献
Burton, Donald J.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 339 - 358
反应条件
sodium hydroxide; dihydrogen peroxide in 1,2,2-trifluoro-trichloroethane
1.) from -5 to -7 deg C, 2 min, 2.) 0 deg C;
参考文献
Chengxue, Zhao; Renmo, Zhou; Heqi, Pan; Xiangshan, Jin; Yangling, Qu; et al.
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 2009 - 2013
