二乙基二硫代氨基甲酸钠(三水)合成路线 （共 16 条）
反应条件
hydrogenchloride in water according to: F. W. Moore and M. L. Larson, Inorg. Chem. 1967, 6, 998., adding HCl; filtn., washing (H2O), drying, recrystallization (Et2O, benzene);
参考文献
Arzoumanian, Henri; Krentzien, Heinz; Corao, Carolina; Lopez, Rafael; Agrifoglio, Giuseppe
Polyhedron, 1995 , vol. 14, p. 2887 - 2892
反应条件
HNO3 in water a soln. of Na comp. slowly added to a soln. of molybdate with strong stirring, pH kepted at about 2 (1 M HNO3); ppt. filtered, washed (water), dried (vac.), recrystd. (benzene:hexane 1:1); elem. anal.;
参考文献
Riveros, Pablo C.; Perilla, Isabel C.; Poveda, Arnulfo; Keller, Heimo J.; Pritzkow
Polyhedron, 2000 , vol. 19, # 22-23 p. 2327 - 2335
反应条件
sodium carbonate in methanol; water; toluene
参考文献
Yu, Wanglin; Wu, Weishi; Hudack, Michelle L.; O'Brien, James J.
Patent: US2009/66224 A1, 2009 ;
反应条件
in dichloromethane under N2, stirred for 20 h at room temp.; filtered (NaBF4), solvent volume reduced in vac., dropwise addn. of diethyl ether, pptn. recrystd. (CH2Cl2/Et2O); elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 397, # 1 p. 59 - 68
反应条件
T=30°C; anschliessend mit NaOCl bei pH 12-12.5;
参考文献
Smith et al.
Journal of Organic Chemistry, 1949 , vol. 14, p. 942
反应条件
in not given prepared according to O. F. Z. Khan, P. O'Brien, Polyhedron, 1991, 10, 325;
参考文献
Sun, Jianwei; Buhro, William E.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 17 p. 3215 - 3218
反应条件
nitric acid in water T=20°C; pH=6 - 10; 0.166667 h;
参考文献
Costa Jr.; Ondar; Versiane; Ramos; Santos; Martin; Raniero; Bussi; Tellez Soto
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2013 , vol. 105, p. 251 - 258
反应条件
in not given prepared according to T. Trindade, P. O'Brien, X.-M. Zhang, M. Motevalli, J. Mater. Chem., 1997, 7, 1011;
参考文献
Sun, Jianwei; Buhro, William E.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 17 p. 3215 - 3218
反应条件
in water SnCl2*2H2O and Na-salt were dissolved in H2O, stirred for 30 min at roomtemp.; filtered, dried in vacuo;
参考文献
Barone, Giampaolo; Chaplin, Tracy; Hibbert, Thomas G.; Kana, Aliki T.; Mahon, Mary F.; Molloy, Kieran C.; Worsley, Ian D.; Parkin, Ivan P.; Price, Louise S.
Journal of the Chemical Society. Dalton Transactions, 2002 , # 6 p. 1085 - 1092
参考文献
Sahasrabudhey; Radhakrishnan
Journal of the Indian Chemical Society, 1954 , vol. 31, p. 853,855
