二乙基二硫代氨基甲酸钠(三水)合成路线 （共 16 条）
反应条件
in ethanol
prepn. from CrCl3*6H2O and Na(C2H5)2NCS2*3H2O in ethanol at elevated temp.;;
参考文献
Gmelin Handbook: Cr: MVol.C, 185, page 404 - 406
反应条件
in water
byproducts: NaCl; stoich. mixt.; Polyhedron, 1999, vol. 18, pp. 3401-3406; dissolved in hot chlorobenzene, filtered to remove Na compd., evapd., elem. anal.;
参考文献
Konarev, Dmitri V.; Kovalevsky, Andrey Y.; Khasanov, Salavat S.; Saito, Gunzi; Lopatin, Dmitri V.; Umrikhin, Alexey V.; Otsuka, Akihiro; Lyubovskaya, Rimma N.
European Journal of Inorganic Chemistry, 2006 , # 9 p. 1881 - 1895
反应条件
in water
room temp.; ppt. was filtered off;
参考文献
Battan, Laura; Fantasia, Serena; Manassero, Mario; Pasini, Alessandro; Sansoni, Mirella
Inorganica Chimica Acta, 2005 , vol. 358, # 3 p. 555 - 564
反应条件
in water
mixing of solns. in stoichiom. amts. (40°C; pptn.); filtration, washing (H2O), air drying, recryst. (CHCl3/hexane), column chromy. (benzene/heptane), zone sublimation (vac., 250°C);
参考文献
Sysoev; Morozova; Zharkova; Igumenov; Semyannikov; Grankin
Journal of Thermal Analysis and Calorimetry, 1998 , vol. 53, # 1 p. 87 - 96
参考文献
Cornock, Margaret C.; Stephenson, T. Anthony
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1977 , p. 501 - 505
参考文献
Sahasrabudhey; Radhakrishnan
Journal of the Indian Chemical Society, 1954 , vol. 31, p. 853,855
