(E,E)-3,3'-硫代二丙烯酸二乙酯合成路线 (共 3 条)
反应条件
sodium perchlorate in N,N-dimethyl-formamide
Ambient temperaturecathode: S-C, working potencial: -0.9 V, current intensity at the beginning: 200 mA;
参考文献
Guillanton, Georges Le; Do, Quang Tho; Simonet, Jacques
Tetrahedron Letters, 1986 , vol. 27, # 20 p. 2261 - 2262
反应条件
1: CS2, NH3 / ethanol
2: 150 °C / 100 Torr
View Scheme
参考文献
Kishida,Y.; Terada,A.
Chemical and Pharmaceutical Bulletin, 1968 , vol. 16, # 7 p. 1351 - 1359
反应条件
1: thiourea / ethanol
2: 150 °C / 100 Torr
View Scheme
参考文献
Kishida,Y.; Terada,A.
Chemical and Pharmaceutical Bulletin, 1968 , vol. 16, # 7 p. 1351 - 1359