4-溴-5-硝基-1,2-苯二甲腈合成路线 （共 4 条）
反应条件
1: 79 percent / conc. H2SO4, conc. HNO3 / 5 h / 20 °C 2: NH4OH / diethyl ether / 48 h 3: 5.6 g / SOCl2 / dimethylformamide / 4 h / 20 - 25 °C View Scheme
参考文献
Shishkina; Maizlish; Shaposhnikov; Lyubimtsev; Smirnov; Baran'ski
Russian Journal of General Chemistry, 1997 , vol. 67, # 5 p. 789 - 792
反应条件
1: NH4OH / diethyl ether / 48 h 2: 5.6 g / SOCl2 / dimethylformamide / 4 h / 20 - 25 °C View Scheme
参考文献
Shishkina; Maizlish; Shaposhnikov; Lyubimtsev; Smirnov; Baran'ski
Russian Journal of General Chemistry, 1997 , vol. 67, # 5 p. 789 - 792
反应条件
triethylamine in isopropyl alcohol 2 h; Heating;
参考文献
Abramov; Smirnov; Abramova; Ivanovskii; Belysheva
Chemistry of Heterocyclic Compounds, 2002 , vol. 38, # 5 p. 576 - 580
反应条件
triethylamine in N,N-dimethyl-formamide T=80°C; 3.33333 h;
参考文献
Dolotova, Olga; Konarev, Alexandr; Volkov, Konstantin; Negrimovsky, Vladimir; Kaliya, Oleg L.
Journal of Porphyrins and Phthalocyanines, 2012 , vol. 16, # 7-8 p. 946 - 957
