1,3-二氧戊环-2-硫酮合成路线 （共 4 条）
反应条件
in toluene 1 h; Heating;
参考文献
Kim, Sunggak; Yi, Kyu Yang
Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2613 - 2615
反应条件
in benzene addition of CSCl2 to germanium dioxolane (benzene, 0°C, N2 or Ar); concn. of solvent, distillation (vac.), elem. anal.;
参考文献
Dousse, G.; Lavayssiere, H.; Satge, J.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1989 , vol. 19, p. 49 - 74
反应条件
in diethyl ether addn. of CSCl2 to Ge-dioxolane (ether, 20°C, N2 or Ar); concn. of solvent, distillation (vac.), elem. anal.;
参考文献
Dousse, G.; Lavayssiere, H.; Satge, J.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1989 , vol. 19, p. 49 - 74
反应条件
(i) Bu3SnNEt2, (ii) /BRN= 1236854/; Multistep reaction;
参考文献
Sakai,S. et al.
Organometallics in Chemical Synthesis, 1970 , vol. 1, p. 45 - 55
