phenyllithium in diethyl ether addn. of PhLi at -30°C to Mes2BF and thiazole (1:1) in Et2O, gradual warming to room temp.; chromy. (SiO2; benzene/hexane);
参考文献
Okada, Keiji; Suzuki, Riho; Oda, Masaji
Journal of the Chemical Society, Chemical Communications, 1995 , # 20 p. 2069 - 2070
in toluene
a soln. of (mes)2BOH added drowpise at room temp. to a stirred soln. of ZnMe2, dild. with toluene, stirred overnight at room temp., refluxed for5 h; evapd., recrystd. (toluene), crystals sepd. manually;
参考文献
Cole, Sarah C.; Coles, Martyn P.; Hitchcock, Peter B.
Journal of the Chemical Society. Dalton Transactions, 2003 , # 19 p. 3663 - 3664
