2',3'-二-O-甲基-腺苷合成路线 （共 7 条）
反应条件
bis(acetylacetonate)nickel(II) in N,N-dimethyl-formamide
T=70°C; 1 h; Further byproducts given;
参考文献
Yamauchi, Kiyoshi; Nakagima, Toru; Kinoshita, Masayoshi
Journal of Organic Chemistry, 1980 , vol. 45, # 19 p. 3865 - 3868
反应条件
in N-methyl-acetamide; methanol; water; mineral oil
参考文献
Nippon Zoki Pharmaceutical Co., Ltd.
Patent: US5705491 A1, 1998 ;
US 5705491 A
反应条件
in methanol; N,N-dimethyl-formamide
T=70°C; 1 h; Title compound not separated from byproducts;
参考文献
Yamauchi, Kiyoshi; Nakagima, Toru; Kinoshita, Masayoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2787 - 2792
反应条件
copper acetylacetonate in N,N-dimethyl-formamide
T=70°C; 0.5 h; reaction without copper(II) acetylacetonate; Product distribution;
参考文献
Yamauchi, Kiyoshi; Hattori, Kazue; Kinoshita, Masayoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1327 - 1330
反应条件
in N,N-dimethyl-formamide
T=70°C; 0.5 h; Further byproducts given;
参考文献
Yamauchi, Kiyoshi; Hattori, Kazue; Kinoshita, Masayoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1327 - 1330
反应条件
in N,N-dimethyl-formamide
T=70°C; 0.5 h; reaction with copper(II) acetylacetonate; Product distribution;
参考文献
Yamauchi, Kiyoshi; Hattori, Kazue; Kinoshita, Masayoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1327 - 1330
反应条件
copper acetylacetonate in N,N-dimethyl-formamide
T=70°C; 1 h; Product distribution;
参考文献
Yamauchi, Kiyoshi; Nakagima, Toru; Kinoshita, Masayoshi
Journal of Organic Chemistry, 1980 , vol. 45, # 19 p. 3865 - 3868
