2,6-二甲氧基苯甲酸甲酯合成路线 （共 22 条）
反应条件
1) K 1) THF, RT, 24h, 2) THF, -30 deg C, 3h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 55, # 19 p. 5386 - 5390
反应条件
1: KOH-solution 2: hydrochloric acid View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 121, p. 262
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 124, p. 320
反应条件
methanol; diethyl ether
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 121, p. 262
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 124, p. 320
参考文献
Journal of the Chemical Society, , vol. 107, p. 841
参考文献
Journal of the Chemical Society, , vol. 107, p. 841
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gazzetta Chimica Italiana, , vol. 111, # 3/4 p. 123 - 128
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gazzetta Chimica Italiana, , vol. 111, # 3/4 p. 123 - 128
反应条件
1: 69 percent / LiAlH4 / tetrahydrofuran / 1 h 2: 65 percent / manganese oxide / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Tsuchida, Eishun; Hasegawa, Etsuo; Komatsu, Teruyuki; Nakata, Taisaku; Nishide, Hiroyuki
Chemistry Letters, 1990 , # 3 p. 389 - 392
反应条件
1: 94 percent / diethyl ether / 0.17 h / Heating 2: 98 percent / glacial HOAc / 2 h / Heating 3: 97 percent / H2 / 5percent Pd/C / diethyl ether / 19 h / 2068.6 Torr 4: m-CPBA / CH2Cl2 / Ambient temperature 5: 88 percent / K2CO3 / acetone / 120 h / Heating 6: 88 percent / KBr, 18-crown-6, m-CPBA / CH2Cl2 / 0.5 h View Scheme
参考文献
Burnell, Robert H.; Caron, Stephane
Canadian Journal of Chemistry, 1992 , vol. 70, # 5 p. 1446 - 1454
反应条件
1: With boron trichloride in dichloromethane T=0°C; 21.5 h; 2: Solvolysis;
参考文献
Biagetti, Matteo; Bellina, Fabio; Carpita, Adriano; Stabile, Paolo; Rossi, Renzo
Tetrahedron, 2002 , vol. 58, # 25 p. 5023 - 5038
