H2SO4 in neat (no solvent) heating (140°C), heating (180-200°C); feeding through condenser (15°C) and absorbtions tube (boric anhydride interspaced with glass wool), condensation (-196°C);
参考文献
Olandi, M.; Bauder, A.
Journal of Chemical Physics, 1987 , vol. 86, p. 624 - 628
boron trichloride room temp.; compn. of react. mixt. followed by IR spectrum;
参考文献
Coyle, T. D.; Cooper, J.; Ritter, J. J.
Inorganic Chemistry, 1968 , vol. 7, p. 1014 - 1020
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Gmelin Handbook: B: B-Verb.9, 1.2.1.4, page 13 - 14
