反应条件
in diethyl ether; toluene Ar atmosphere; to suspn. of CpZrCl3DME in 3:1 toluene-diethyl ether at -78 °C diethyl ether soln. of LiC9H7 was added, stirred and allowed to warm to room temp. over 8 h; solvent removed under reduced pressure, residue extd. with CH2Cl2, suspn. cooled to -10 °C for 1 h, filtered, filtrate concd., pentane added, cooled to -18 °C for 12 h, filtered, filtrate concd., pentane added; elem. anal.;
参考文献
Alcock, Nathaniel W.; Clase, Howard J.; Duncalf, David J.; Hart, Suzanne L.; McCamley, Andrew; McCormack, Peter J.; Taylor, Paul C.
Journal of Organometallic Chemistry, 2000 , vol. 605, # 1 p. 45 - 54
