反应条件
1: ammonia 2: acid 3: 89 percent / K2CO3, NaI, CuI / dimethylformamide / 12 h 4: 92 percent / CBr4, PPh3 / CH2Cl2 / 1 h / Ambient temperature 5: 89 percent / K2CO3, NaI, CuI / dimethylformamide / 40 °C 6: 65 percent / H2, (CH2NH2)2 / P-2 Ni / ethanol 7: 98 percent / LiOH, H2O / tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) r.t., 12 h View Scheme
参考文献
Durand, Sandrine; Parrain, Jean-Luc; Santelli, Maurice
Synthesis, 1998 , # 7 p. 1015 - 1018
