2-(3-硝基苯基)环氧乙烷合成路线 （共 12 条）
反应条件
2: 1.) HCOOH, 2.) CF3CO3H, TFA 3: SnCl2 View Scheme
参考文献
Archer, Sydney; Glick, Stanley D.; Maisonneuve, Isabelle M.; Bidlack, Jean M.; Xu, Jimmy Y.; Teitler, Milt; Sebastian, Alice; El-Hamouly, Wageeh; Hutchinson, Ian
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 10 p. 1139 - 1144
反应条件
hexafluoroisopropyl alcohol; hydroxy(phenyl)(tetrafluoroborato)-λ3-iodane in dichloromethane; water T=20°C; 42 h;
参考文献
Miyamoto, Kazunori; Tada, Norihiro; Ochiai, Masahito
Journal of the American Chemical Society, 2007 , vol. 129, # 10 p. 2772 - 2773
反应条件
ammonia; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in water; acetonitrile T=70°C;
参考文献
Deshmukh, Swapnil S.; Huddar, Sameerana N.; Jadhav, Ravindra R.; Akamanchi, Krishnacharya G.
Tetrahedron Letters, 2011 , vol. 52, # 35 p. 4533 - 4536
反应条件
1: 63 percent / ethanol / Heating 2: H2 / Ni / methanol / Ambient temperature View Scheme
参考文献
Alpatova, T. A.; Kulinskii, V. I.; Yashunskii, V. G.
Pharmaceutical Chemistry Journal, 1983 , vol. 17, # 8 p. 543 - 546
Khimiko-Farmatsevticheskii Zhurnal, 1983 , vol. 17, # 8 p. 922 - 925
反应条件
1: 80 percent / ethanol / Heating 2: H2 / Ni / methanol / Ambient temperature 3: sodium nitrite / aq. H2SO4 / 0 °C 4: aq. H2SO4 / Heating View Scheme
参考文献
Alpatova, T. A.; Kulinskii, V. I.; Yashunskii, V. G.
Pharmaceutical Chemistry Journal, 1983 , vol. 17, # 8 p. 543 - 546
Khimiko-Farmatsevticheskii Zhurnal, 1983 , vol. 17, # 8 p. 922 - 925
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran T=0 - 20°C; 48 h;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
[(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(III) acetate; water in tetrahydrofuran T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
boron trifluoride diethyl etherate in diethyl ether
T=20°C; 0.5 h;
参考文献
Rao, D. Chandra; Reddy, D. Kumar; Shekhar; Chinababu; Rao, Ch. Bhujanga; Venkateswarlu
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014 , vol. 53, # 3 p. 356 - 358
