5,6,7,8-四氢-1,8-萘啶-2-丙胺合成路线 （共 12 条）
反应条件
ammonium hydroxide; hydrogen; nickel T=50°C; P=2068.59 Torr; 16 h;
参考文献
Yasuda, Nobuyoshi; Hsiao; Jensen, Mark S; Rivera, Nelo R; Yang, Chunhua; Wells, Kenneth M; Yau, James; Palucki, Michael; Tan, Lushi; Dormer, Peter G; Volante, Ralph P; Hughes, David L; Reider, Paul J
The Journal of organic chemistry, 2004 , vol. 69, # 6 p. 1959 - 1966
反应条件
sodium amide in toluene T=90°C; Chichibabin reaction; 15 h;
参考文献
Palucki, Michael; Hughes, David L; Yasuda, Nobuyoshi; Yang, Chunhua; Reider, Paul J
Tetrahedron Letters, 2001 , vol. 42, # 39 p. 6811 - 6814
反应条件
hydrogenchloride T=40°C;
参考文献
Yasuda, Nobuyoshi; Hsiao; Jensen, Mark S; Rivera, Nelo R; Yang, Chunhua; Wells, Kenneth M; Yau, James; Palucki, Michael; Tan, Lushi; Dormer, Peter G; Volante, Ralph P; Hughes, David L; Reider, Paul J
The Journal of organic chemistry, 2004 , vol. 69, # 6 p. 1959 - 1966
反应条件
1: aq. NaOH / tetrahydrofuran / 20 °C 2: 89 percent / H2; aq. NH4OH / Raney Ni / 16 h / 50 °C / 2068.59 Torr View Scheme
参考文献
The Journal of organic chemistry, , vol. 69, # 6 p. 1959 - 1966
反应条件
1: 92 percent / H2 / PtO2 / ethanol / 18 h / 20 °C / 760 Torr 2: aq. HCl / 2.5 h / 85 °C 3: aq. NaOH / tetrahydrofuran / 20 °C 4: 89 percent / H2; aq. NH4OH / Raney Ni / 16 h / 50 °C / 2068.59 Torr View Scheme
参考文献
The Journal of organic chemistry, , vol. 69, # 6 p. 1959 - 1966
反应条件
1: aq. HCl / 2.5 h / 85 °C 2: aq. NaOH / tetrahydrofuran / 20 °C 3: 89 percent / H2; aq. NH4OH / Raney Ni / 16 h / 50 °C / 2068.59 Torr View Scheme
参考文献
The Journal of organic chemistry, , vol. 69, # 6 p. 1959 - 1966
反应条件
1: NaOH / methanol; H2O / 16.5 h / 40 - 50 °C 2: 85 percent / H2 / Rh/C / methanol / 10 h / 5 °C / 2068.59 Torr 3: 100 percent / aq. HCl / 40 °C View Scheme
参考文献
The Journal of organic chemistry, , vol. 69, # 6 p. 1959 - 1966
反应条件
1: H2 / Pd/Al2O3 / methanol / 25 h / 10 - 24 °C / 2068.59 Torr 2: 98.8 percent Chromat. / aq. HCl / 1 h / 90 °C 3: 90 percent / NaNH2 / toluene / 7 h / 90 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 25 p. 8723 - 8730
反应条件
1: 85 percent / H2 / Rh/C / methanol / 10 h / 5 °C / 2068.59 Torr 2: 100 percent / aq. HCl / 40 °C View Scheme
参考文献
The Journal of organic chemistry, , vol. 69, # 6 p. 1959 - 1966
反应条件
1: 98.8 percent Chromat. / aq. HCl / 1 h / 90 °C 2: 90 percent / NaNH2 / toluene / 7 h / 90 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 25 p. 8723 - 8730
