4,5-双(苯基甲氧基)-1,2-苯二甲腈合成路线 (共 7 条)
反应条件
in N,N-dimethyl-formamide T=150°C; 8 h;
参考文献
Cabezon, Beatriz; Quesada, Ernesto; Esperanza, Sagrario; Torres, Tomas
European Journal of Organic Chemistry, 2000 , # 15 p. 2767 - 2775
反应条件
1: 54 percent / KOH / dimethylsulfoxide / 8 h / -20 °C 2: dimethylformamide / 8 h / Heating View Scheme
参考文献
Russian Chemical Bulletin, , vol. 54, # 9 p. 2094 - 2098
反应条件
1: 90 percent / 84percent aq. KOH, Aliquate 336 / dimethylformamide / 4 h / 120 °C 2: 92 percent / Br2 / CH2Cl2 / 3 h / 0 - 20 °C 3: 60 percent / dimethylformamide / 8 h / 150 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 41, # 11 p. 1789 - 1802
反应条件
1: 92 percent / Br2 / CH2Cl2 / 3 h / 0 - 20 °C 2: 60 percent / dimethylformamide / 8 h / 150 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 41, # 11 p. 1789 - 1802
反应条件
1: 90 percent / 84percent aq. KOH, Aliquate 336 / dimethylformamide / 4 h / 120 °C 2: 92 percent / Br2 / CH2Cl2 / 3 h / 0 - 20 °C 3: 60 percent / dimethylformamide / 8 h / 150 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 41, # 11 p. 1789 - 1802
反应条件
1: 54 percent / KOH / dimethylsulfoxide / 8 h / -20 °C 2: dimethylformamide / 8 h / Heating View Scheme
参考文献
Russian Chemical Bulletin, , vol. 54, # 9 p. 2094 - 2098
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate T=20°C; Catalytic hydrogenation; debenzylation; 4 h;
参考文献
Cabezon, Beatriz; Quesada, Ernesto; Esperanza, Sagrario; Torres, Tomas
European Journal of Organic Chemistry, 2000 , # 15 p. 2767 - 2775