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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
207128-57-2
合成路线
（共 9 条）
120122-47-6
1-甲基-4-硝基-2-(三氟乙酰)-1H-吡咯
→
反应条件
207128-57-2
反应条件
1: 78 percent / triethylamine / tetrahydrofuran / 16 h / Ambient temperature 2: 910 mg / hydrogen / PtO2 / methanol / 1 h / Ambient temperature 3: 54 percent / 4-(dimethylamino)pyridine / acetonitrile / 16 h / Ambient temperature View Scheme
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
190835-32-6
+
207128-68-5
→
反应条件
207128-57-2
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile 16 h; Ambient temperature;
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
207128-83-4
→
反应条件
207128-57-2
反应条件
1: 78 percent / triethylamine / tetrahydrofuran / 16 h / Ambient temperature 2: 910 mg / hydrogen / PtO2 / methanol / 1 h / Ambient temperature 3: 54 percent / 4-(dimethylamino)pyridine / acetonitrile / 16 h / Ambient temperature View Scheme
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
207128-72-1
→
反应条件
207128-57-2
反应条件
1: 952 mg / hydrogen / PtO2 / methanol / 1 h / Ambient temperature; other catalyst: Pd-C 2: 78 percent / triethylamine / tetrahydrofuran / 16 h / Ambient temperature 3: 910 mg / hydrogen / PtO2 / methanol / 1 h / Ambient temperature 4: 54 percent / 4-(dimethylamino)pyridine / acetonitrile / 16 h / Ambient temperature View Scheme
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
207128-73-2
→
反应条件
207128-57-2
反应条件
1: 910 mg / hydrogen / PtO2 / methanol / 1 h / Ambient temperature 2: 54 percent / 4-(dimethylamino)pyridine / acetonitrile / 16 h / Ambient temperature View Scheme
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
1644-82-2
2-氟-6-硝基苯甲醛
→
反应条件
207128-57-2
反应条件
1: 74 percent / dimethylformamide / 2 h / 120 °C 2: 88 percent / potassium carbonate / dimethylformamide / 1 h / 60 °C 3: 85 percent / hydrochloric acid / 1 h / 60 °C 4: 78 percent / pyridine / acetonitrile / 16 h / Ambient temperature 5: 54 percent / 4-(dimethylamino)pyridine / acetonitrile / 16 h / Ambient temperature View Scheme
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
28484-86-8
→
反应条件
207128-57-2
反应条件
1: 74 percent / dimethylformamide / 2 h / 120 °C 2: 88 percent / potassium carbonate / dimethylformamide / 1 h / 60 °C 3: 85 percent / hydrochloric acid / 1 h / 60 °C 4: 78 percent / pyridine / acetonitrile / 16 h / Ambient temperature 5: 54 percent / 4-(dimethylamino)pyridine / acetonitrile / 16 h / Ambient temperature View Scheme
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
207128-65-2
→
反应条件
207128-57-2
反应条件
1: 88 percent / potassium carbonate / dimethylformamide / 1 h / 60 °C 2: 85 percent / hydrochloric acid / 1 h / 60 °C 3: 78 percent / pyridine / acetonitrile / 16 h / Ambient temperature 4: 54 percent / 4-(dimethylamino)pyridine / acetonitrile / 16 h / Ambient temperature View Scheme
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
207128-66-3
→
反应条件
207128-57-2
反应条件
1: 85 percent / hydrochloric acid / 1 h / 60 °C 2: 78 percent / pyridine / acetonitrile / 16 h / Ambient temperature 3: 54 percent / 4-(dimethylamino)pyridine / acetonitrile / 16 h / Ambient temperature View Scheme
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
