1: With magnesium in anhydrous butyl ether
2 h; RefluxInert atmosphere;
2: With water-d2 in anhydrous butyl ether
T=-10.16°C;
参考文献
Calladine, James A.; Duckett, Simon B.; George, Michael W.; Matthews, Steven L.; Perutz, Robin N.; Torres, Olga; Vuong, Khuong Q.
Journal of the American Chemical Society, 2011 , vol. 133, # 7 p. 2303 - 2310