5-氨基-1,3-苯二酚合成路线 （共 14 条）
反应条件
1: aqueous dioxane
2: aqueous NaOH
View Scheme
参考文献
Sorm; Novotny
Chemicke Listy, 1954 , vol. 49, p. 901,907
Collection of Czechoslovak Chemical Communications, 1955 , vol. 20, p. 1206,1212
Chem. Zentralbl., 1955 , vol. 126, p. 13244
反应条件
1: With hydrogenchloride in water
2: With sulfuric acid; sodium nitrite in water
T=0°C; Sandmeyer reaction; 0.25 h;
3: With potassium iodide in water; ethyl acetate
Sandmeyer reaction; 7 h;
参考文献
Morales-Serna, Jose Antonio; Zuniga-Martinez, Armando; Salmon, Manuel; Gavino, Ruben; Cardenas, Jorge
Synthesis, 2012 , vol. 44, # 3 art. no. M89011SS, p. 446 - 452
反应条件
potassium acetate; acetic acid
1.5 h; Reflux;
参考文献
Peterca, Mihai; Imam, Mohammad R.; Ahn, Cheol-Hee; Balagurusamy, Venkatachalapathy S. K.; Wilson, Daniela A.; Rosen, Brad M.; Percec, Virgil
Journal of the American Chemical Society, 2011 , vol. 133, # 7 p. 2311 - 2328
参考文献
Pollak
Monatshefte fuer Chemie, 1893 , vol. 14, p. 403
