反应条件
1: 95 percent / H2 / Lindlar's catalyst/quinoline / hexane 2: 90 percent / PBr3, pyridine / diethyl ether / cooled, 30 min, then standing overnight, then reflux, 2 h 3: 70 percent / benzene; dimethylformamide / 16 h / Heating 4: 80 percent / NaCl / H2O; dimethylsulfoxide / 8 h / 140 - 145 °C 5: 90 percent / LiAlH4 / diethyl ether / reflux, then room temp., overnight, then reflux, 30 min 6: 90 percent / PBr3, pyridine / diethyl ether / reflux, 20 min, then room temp., overnight, then reflux, 2 h 7: 1)Mg / 1)THF 2)room temp., overnight, then reflux, 3 h 8: 60 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature View Scheme
参考文献
Vig, O. P.; Sharma, M. L.; Verma, N. K.; Malik, Neera
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 11 p. 950 - 951
