2-甲氧基-5-(3′,7′-二甲基辛基氧基)对苯二甲醛合成路线 （共 2 条）
反应条件
1: 1,4-dibromo-2-(3,7-dimethyloctyloxy)-5-methoxybenzene With n-butyllithium in diethyl ether; hexane T=-10°C; 0.0833333 h; 2: N,N-dimethyl-formamide in diethyl ether; hexane T=20°C; 1 h; Further stages.;
参考文献
Ramos; Rispens; Van Duren; Hummelen; Janssen
Journal of the American Chemical Society, 2001 , vol. 123, # 27 p. 6714 - 6715
反应条件
1.1: 75 percent / Br2 / acetic acid / 2 h / 65 - 116 °C 2.1: n-butyllithium / diethyl ether; hexane / 0.08 h / -10 °C 2.2: 56 percent / diethyl ether; hexane / 1 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 123, # 27 p. 6714 - 6715
