1-[(2-氯乙基)硫代]-4-甲苯合成路线 （共 14 条）
反应条件
1: para-thiocresol With sodium ethanolate in ethanol T=20°C; Metallation; 0.5 h; 2: 2-chloro-ethanol in ethanol Alkylation; 3.5 h; Heating; 3: With hydrogenchloride in ethanol; water Chlorination; 15 h, r.t., 4.5 h, reflux;
参考文献
Van Der Schaaf, Paul A.; Kolly, Roman; Kirner, Hans-Juerg; Rime, Francois; Muehlebach, Andreas; Hafner, Andreas
Journal of Organometallic Chemistry, 2000 , vol. 606, # 1 p. 65 - 74
反应条件
pyridine; thionyl chloride
参考文献
Fromm; Kohn
Chemische Berichte, 1921 , vol. 54, p. 323
参考文献
Gilman; Beaber
Journal of the American Chemical Society, 1925 , vol. 47, p. 1451
反应条件
1: carbon tetrachloride; chlorine 2: carbon tetrachloride View Scheme
参考文献
Padmavathi, Venkatapuram; Venkatesh, Bhumireddy Chinnachennaiahgari; Premakumari, Chokkappagari; Padmaja, Adivireddy
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 3 p. 646 - 651
反应条件
magnesium in tetrahydrofuran; diethyl ether 1 h; Ambient temperature;
参考文献
Bauld, Nathan L.; Aplin, J. Todd; Yueh, Wang; Endo, Stephanie; Loving, Angie
Journal of Physical Organic Chemistry, 1998 , vol. 11, # 1 p. 15 - 24
参考文献
Lecher
Chemische Berichte, 1925 , vol. 58, p. 415
反应条件
potassium tert-butylate
参考文献
Bird,R.; Stirling,J.M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1973 , p. 1221 - 1226
参考文献
Fromm; Kohn
Chemische Berichte, 1921 , vol. 54, p. 323
参考文献
Lecher
Chemische Berichte, 1925 , vol. 58, p. 415
反应条件
aluminium trichloride; benzene
参考文献
Klamann; Bertsch
Chemische Berichte, 1955 , vol. 88, p. 1226,1232
