sec.-butyllithium; (-)-sparteine in diethyl ether sec-BuLi was added to soln. of sparteine and pyrrolidine at -78°C; reaction time 4-6 h; addn. of tin-compound soln.; warming to room temperature (3 h);; flash chromatography with ethyl acetate/hexane; (1)H-and (13)C-NMR; elem. anal.;
参考文献
Kerrick, Shawn T.; Beak, Peter
Journal of the American Chemical Society, 1991 , vol. 113, # 25 p. 9708 - 9710