1: 4-nitro-aniline With tetrafluoroboric acid; sodium nitrite in water T=0°C; 0.666667 h; 2: 1-(4-methoxyphenyl)ethenyl acetate With [Ru(II)(2,2’-bipyridine)3]Cl2 in N,N-dimethyl-formamide T=20°C; 2 h; Irradiation;
1: With trifluoroacetic anhydride T=80°C; 2: With bismuth trifluoromethanesulphonate T=80°C; Friedel-Crafts reaction; Title compound not separated from byproducts;
参考文献
Wilkinson, Mark C.; Saez, Fabienne; Wei, Lee Hon
Synlett, 2006 , # 7 p. 1063 - 1066
