4-(3-甲氧基苯基)-3-丁烯-2-酮合成路线 （共 4 条）
反应条件
1: 73 percent / H2; HOAc / Pd/C / ethanol / 24 h 2: 44 percent / NH2OH*HCl; pyridine / ethanol / 24 h 3: 5 percent / (CF3CO)2O; 4-chloranil / CH2Cl2 / 22 h / 20 °C View Scheme
参考文献
Kitamura, Mitsuru; Yoshida, Masayuki; Kikuchi, Takashi; Narasaka, Koichi
Synthesis, 2003 , # 15 p. 2415 - 2426
反应条件
1: 73 percent / H2; HOAc / Pd/C / ethanol / 24 h 2: 44 percent / NH2OH*HCl; pyridine / ethanol / 24 h 3: 83 percent / (CF3CO)2O; 4-chloranil / CH2Cl2 / 22 h / 20 °C View Scheme
参考文献
Kitamura, Mitsuru; Yoshida, Masayuki; Kikuchi, Takashi; Narasaka, Koichi
Synthesis, 2003 , # 15 p. 2415 - 2426
反应条件
1: 73 percent / H2; HOAc / Pd/C / ethanol / 24 h
2: 44 percent / NH2OH*HCl; pyridine / ethanol / 24 h
3: (CF3CO)2O / CH2Cl2 / 24 h / 20 °C
4: 4-chloranil / CH2Cl2 / 21 h / 20 °C
View Scheme
参考文献
Kitamura, Mitsuru; Yoshida, Masayuki; Kikuchi, Takashi; Narasaka, Koichi
Synthesis, 2003 , # 15 p. 2415 - 2426
反应条件
1: 73 percent / H2; HOAc / Pd/C / ethanol / 24 h
2: 44 percent / NH2OH*HCl; pyridine / ethanol / 24 h
3: (CF3CO)2O / CH2Cl2 / 24 h / 20 °C
View Scheme
参考文献
Kitamura, Mitsuru; Yoshida, Masayuki; Kikuchi, Takashi; Narasaka, Koichi
Synthesis, 2003 , # 15 p. 2415 - 2426
