SgcF epoxide hydrolase from the C-1027 biosynthetic gene cluster; H218O T=25°C; pH=8; 8 h; aq. phosphate buffer; optical yield given as percent eeregiospecific reaction;
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Lin, Shuangjun; Horsman, Geoffrey P.; Chen, Yihua; Li, Wenli; Shen, Ben
Journal of the American Chemical Society, 2009 , vol. 131, # 45 p. 16410 - 16417
1: With trimethylaluminum in toluene T=-60 - 20°C; 5.83333 h; Cooling with acetone-dry ice; 2: With sodium sulfate in tetrahydrofuran; water T=20°C; 1.5 h;
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Patent: US2003/233015 A1, 2003 ;
Location in patent: Page 13 ;
1: in toluene T=-60 - 20°C; 5.83333 h; Under nitrogenCooling with acetone-dry ice; 2: With water in tetrahydrofuran; toluene 0.5 h;
参考文献
Arnold, Macklin Brian; Bleisch, Thomas John; Cuff, George William; Ornstein, Paul Leslie; Zimmerman, Dennis Michael
Patent: US2003/225163 A1, 2003 ;
Location in patent: Page 13-14 ;
