双(2,4-二甲氧基苄基)胺合成路线 (共 7 条)
反应条件
sodium tris(acetoxy)borohydride in tetrahydrofuran T=20°C; 2 h;
参考文献
Zakharian, Tatiana Y.; Christianson, David W.
Tetrahedron Letters, 2010 , vol. 51, # 28 p. 3645 - 3648
反应条件
sodium tetrahydroborate; nickel dichloride in ethanol T=20°C; 0.0833333 h;
参考文献
Synthetic Communications, , vol. 32, # 8 p. 1265 - 1269
反应条件
1: 96 percent / NH3 / ethanol / 18 h / Ambient temperature 2: 89 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 9 p. 703 - 708
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Katritzky; Zhao; Hitchings
Synthesis, 1991 , # 9 p. 703 - 708
反应条件
1: H2, NH3 / Raney-Ni / methanol 2: (i) TsOH, toluene, (ii) aq. NaBH4 View Scheme
参考文献
Chemische Berichte, , vol. 101, # 10 p. 3623 - 3641
反应条件
1: magnesium sulfate / ethanol / 4 h / 78 °C 2: sodium tetrahydroborate / ethanol / 20 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 37 p. 7610 - 7617
反应条件
triethylamine in benzene
T=0 - 20°C;
参考文献
Navidpour, Latifeh; Lu, Wallach; Taylor, Scott D.
Organic Letters, 2006 , vol. 8, # 24 p. 5617 - 5620