1-烯丙基四氢-4(1H)-吡啶酮合成路线 (共 4 条)
反应条件
4-(N,N-dimethlyamino)pyridine; [2,2']bipyridinyl; AZADO; copper(l) chloride in acetonitrile T=20°C; 2.5 h; chemoselective reaction;
参考文献
Sasano, Yusuke; Nagasawa, Shota; Yamazaki, Mai; Shibuya, Masatoshi; Park, Jaiwook; Iwabuchi, Yoshiharu
Angewandte Chemie - International Edition, 2014 , vol. 53, # 12 p. 3236 - 3240
Angew. Chem., 2014 , vol. 126, # 12 p. 3300 - 3304,5
反应条件
1: toluene / 4 h / Heating 2: 100.7 g / aq. HCl / 12 h / Heating View Scheme
参考文献
Synthesis, , # 3 p. 364 - 366
反应条件
1: potassium carbonate / ethanol / 4 h / 0 - 20 °C / |Inert atmosphere 2: 4-(N,N-dimethlyamino)pyridine; [2,2']bipyridinyl; AZADO; copper(l) chloride / acetonitrile / 2.5 h / 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 12 p. 3236 - 3240
Angew. Chem., , vol. 126, # 12 p. 3300 - 3304,5
反应条件
hydrogenchloride 12 h; Heating;
参考文献
Miyahara; Goto; Inazu
Synthesis, 2001 , # 3 p. 364 - 366