in neat (no solvent) byproducts: hydrogen; introduction of n-BuNH2*BH3 under N2 into flask; heating in an oil bath by slow raising the temp. to 120°C for 30 min; heating at this temp. for 1 h; heating at 200°C for 1 h; distn. in vac.;

in not given byproducts: H2; thermal decomposition between 40 and 50°C;;

tetrabutylmercaptodiborane

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