N,N-二甲基三甲基硅胺合成路线 （共 111 条）
反应条件
in neat (no solvent)
byproducts: Me3SiCl; under N2, equimolar amt. of Me3SiNMe2 was added to stirred (Me3Si)2NB(CH(CH3)2)Cl at 0°C, warmed to room temp., stirred overnight; Me3SiCl removed under vac., distd.;
参考文献
Li, Bei-Li; Goodman, Mary A.; Neilson, Robert H.
Inorganic Chemistry, 1984 , vol. 23, p. 1368 - 1371
反应条件
in tetrahydrofuran
T=20°C; 1.5 h;
参考文献
Schmidt, Joerg Christoph; Adiwidjaja, Gunadi; Schaumann, Ernst
Arkivoc, 2012 , vol. 2012, # 3 p. 104 - 109
反应条件
in dichloromethane
10 h; Heating;
参考文献
Seitz, Gunther; The, Han-Sui
Synthesis, 1984 , # 2 p. 119 - 121
反应条件
trimethylsilyl trifluoromethanesulfonate
0.5 h;
参考文献
Combret, Jean-Claude; Klein, Jean-Louis; Mouslouhouddine, Mohamed
Tetrahedron Letters, 1984 , vol. 25, # 32 p. 3449 - 3452
反应条件
in benzene
at 80°C for 30 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.7.1, page 104 - 132
反应条件
sodium iodide in acetonitrile
0.5 h; Ambient temperature;
参考文献
Arend, Michael; Risch, Nikolaus
Synlett, 1997 , vol. 1997, # 8 p. 974 - 976
反应条件
in acetonitrile
Irradiation; Yields of byproduct given;
参考文献
Kirschberg, Thorsten; Mattay, Jochen
Journal of Organic Chemistry, 1996 , vol. 61, # 25 p. 8885 - 8896
反应条件
dinitrogen pentaoxide in dichloromethane
T=-5°C; 0.75 h;
参考文献
Millar, Ross W.; Philbin, Simon P.
Tetrahedron, 1997 , vol. 53, # 12 p. 4371 - 4386
反应条件
methyl iodide in toluene
T=100 - 110°C; 79 h;
参考文献
Yamamoto, Yasushi; Shimizu, Hideaki; Hamada, Yoshitaka
Journal of Organometallic Chemistry, 1996 , vol. 509, # 2 p. 119 - 122
反应条件
(i), (ii) (pyrolysis); Multistep reaction;
参考文献
Matsuda,I. et al.
Journal of Organometallic Chemistry, 1974 , vol. 69, p. 353 - 359
