N,N-二甲基三甲基硅胺合成路线 （共 111 条）
反应条件
1: With B,B',B''-trichlor-N,N',N''-tris-(dichlorboryl)borazine in hexane
T=-78 - 20°C; Inert atmosphere;
2: in dichloromethane
T=-25°C;
参考文献
Anand, Benadir; Noeth, Heinrich; Schwenk-Kircher, Holger; Troll, Alexander
European Journal of Inorganic Chemistry, 2008 , # 20 p. 3186 - 3199
反应条件
B,B',B''-trichlor-N,N',N''-tris-(dichlorboryl)borazine in hexane
T=-78 - 20°C; Inert atmosphere;
参考文献
Anand, Benadir; Noeth, Heinrich; Schwenk-Kircher, Holger; Troll, Alexander
European Journal of Inorganic Chemistry, 2008 , # 20 p. 3186 - 3199
反应条件
1: With B,B',B''-trichlor-N,N',N''-tris-(dichlorboryl)borazine in hexane
T=-78 - 20°C; Inert atmosphere;
2: in dichloromethane
T=-25°C;
参考文献
Anand, Benadir; Noeth, Heinrich; Schwenk-Kircher, Holger; Troll, Alexander
European Journal of Inorganic Chemistry, 2008 , # 20 p. 3186 - 3199
反应条件
in hexane
inert gas; reflux for 3 h;; condensation of the chlorosilane; distillation of the product: 120 ° C/0.01 Torr; elem. anal.;;
参考文献
Fessenbecker, Achim; Hergel, Achim; Hettrich, Ralph; Schaefer, Volker; Siebert, Walter
Chemische Berichte, 1993 , vol. 126, # 10 p. 2205 - 2210
反应条件
in neat (no solvent)
heated to 140°C for 2 d; distn.; elem. anal.;
参考文献
Bonn, Karl-Heinz van; Schreyer, Peter; Paetzold, Peter; Boese, Roland
Chemische Berichte, 1988 , vol. 121, p. 1045 - 1058
参考文献
Noeth, H.
Zeitschrift fuer Naturforschung, 1961 , vol. 16b, p. 618 - 620
反应条件
S4N4Cl2 in acetonitrile
参考文献
Roesky, Herbert W.; Pelz, Cornelia; Gieren, Alfred; Haedicke, Erich
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1981 , vol. 36, # 11 p. 1437 - 1443
反应条件
in chloroform
reflux for 3 d; distn.; elem. anal.;
参考文献
Bonn, Karl-Heinz van; Schreyer, Peter; Paetzold, Peter; Boese, Roland
Chemische Berichte, 1988 , vol. 121, p. 1045 - 1058
参考文献
Noeth, H.
Zeitschrift fuer Naturforschung, 1961 , vol. 16b, p. 618 - 620
参考文献
Noeth, H.
Zeitschrift fuer Naturforschung, 1961 , vol. 16b, p. 618 - 620
