N,N-二甲基三甲基硅胺合成路线 （共 111 条）
反应条件
in benzene at 80°C for 30 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.7.1, page 104 - 132
反应条件
in monofluoro-trichloromethane onto a frozen soln. of Me3SiNMe2 in CFCl3 in an NMR-tube BF3 is condensed at -196°C, warming up to room temp.; monitored by NMR-spectroscopy;
参考文献
Tornieporth-Oetting, I. C.; Klapoetke, T. M.
Polyhedron, 1992 , vol. 11, p. 2183 - 2186
反应条件
in solid matrix onto a frozen soln. of Me3SiNMe2 in SO2 in an NMR-tube AsF5 is condensed at -196°C, warming to room temp.; monitored by NMR-spectroscopy;
参考文献
Tornieporth-Oetting, I. C.; Klapoetke, T. M.
Polyhedron, 1992 , vol. 11, p. 2183 - 2186
反应条件
in solid matrix onto a frozen soln. of Me3SiNMe2 in SO2 in an NMR-tube BF3 is condensed at -196°C, warming up to room temp.; monitored by NMR-spectroscopy;
参考文献
Tornieporth-Oetting, I. C.; Klapoetke, T. M.
Polyhedron, 1992 , vol. 11, p. 2183 - 2186
反应条件
mixing for 2 h, cooling with ice;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.2, page 50 - 76
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 2.2, page 191 - 196
反应条件
room temp., vehement react.;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.2, page 14 - 30
参考文献
Gmelin Handbook: B: B-Verb.4, 4.4.1, page 110 - 117
反应条件
T=120°C; Equilibrium constant;
参考文献
Pace,S.C. et al.
Journal of Organometallic Chemistry, 1973 , vol. 56, p. 141 - 157
参考文献
Appel,R. et al.
Chemische Berichte, 1972 , vol. 105, p. 2492 - 2507
