2-溴-4,6-二-叔-丁基苯酚合成路线 （共 14 条）
反应条件
in ethylene glycol
T=140°C; Duff reaction; 1 h;
参考文献
Vol'eva; Belostotskaya; Komissarova; Kurkovskaya; Pleshakova; Prokofeva
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 10 p. 1488 - 1491
反应条件
diethylamine in tetrahydrofuran
20 h; Heating;
参考文献
Muslin, D. V.; Lyapina, N. Sh.; Klimov, E. S.; Kirilicheva, V. G.; Razuvaev, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 6 p. 998 - 1002
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 6 p. 1385 - 1389
反应条件
1: 2-bromo-4,6-di-tert-butyl-phenol With n-butyllithium
2: chloro-trimethyl-silane
参考文献
Pan, Jun; Su, Mingjuan; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 37 p. 8647 - 8651
反应条件
1: 2-bromo-4,6-di-tert-butyl-phenol With n-butyllithium in diethyl ether; hexane
T=0 - 20°C; 2 h;
2: 2,3-dimethyl-1-indanone in diethyl ether; hexane
3: With hydrogenchloride
Further stages.;
参考文献
Turner, Luke E.; Thorn, Matthew G.; Swartz II; Chesnut, Robert W.; Fanwick, Phillip E.; Rothwell, Ian P.
Dalton Transactions, 2003 , # 24 p. 4580 - 4589
