6-叠氮-6-脱氧-D-葡萄糖合成路线 （共 13 条）
反应条件
1: 91 percent / pyridine / 16 h / -15 °C
2: 92 percent / NaN3 / dimethylformamide / 20 h / 120 °C
3: 82 percent / aq. TFA / 0.5 h / 40 °C
View Scheme
参考文献
Fernandez, Jose M. Garcia; Mellet, Carmen Ortiz; Maciejewski, Sylwester; Defaye, Jacques
Journal of the Chemical Society, Chemical Communications, 1996 , # 24 p. 2741 - 2742
反应条件
1: 92 percent / NaN3 / dimethylformamide / 20 h / 120 °C
2: 82 percent / aq. TFA / 0.5 h / 40 °C
View Scheme
参考文献
Fernandez, Jose M. Garcia; Mellet, Carmen Ortiz; Maciejewski, Sylwester; Defaye, Jacques
Journal of the Chemical Society, Chemical Communications, 1996 , # 24 p. 2741 - 2742
反应条件
1: With hydrogen; palladium 10 on activated carbon in methanol; water
T=20°C; P=1551.49 Torr;
2: With hydrogenchloride
参考文献
Wiebe, Leonard; Diakur, James
Patent: US2007/21380 A1, 2007 ;
Location in patent: Page/Page column 13 ;
