2-苯基-1,2-环氧丙烷合成路线 (共 116 条)
参考文献
Somerville; Spoerri
Journal of the American Chemical Society, 1951 , vol. 73, p. 697
反应条件
ammonium chloride; lithium diisopropyl amide
1.) a) r.t. over night b) reflux, 4 h; Yield given. Multistep reaction;
参考文献
Gajewski,J.J.; Jurayj,J.; Kimbrough,D.R.
Journal of the American Chemical Society, 1987 , vol. 109, p. 1170
反应条件
1: With bis(cyclopentadienyl)titanium dichloride; zinc in tetrahydrofuran; acetonitrile
0.5 h; Inert atmosphere;
2: With sodium dihydrogenphosphate; water in tetrahydrofuran; acetonitrile
0.333333 h; Inert atmosphere;
参考文献
Fernandez-Mateos; Encinas Madrazo; Herrero Teijon; Rubio Gonzalez
Journal of Organic Chemistry, 2009 , vol. 74, # 10 p. 3913 - 3918
反应条件
in toluene
T=50°C; effect of the nickel catalyst and reaction temp.; Product distribution;
参考文献
Miyashita, Akira; Shimada, Takeshi; Sugawara, Atsushi; Nohira, Hiroyuki
Chemistry Letters, 1986 , p. 1323 - 1326
反应条件
dihydrogen peroxide; Ti-beta-Na in acetonitrile
var. of catalyst, solvent, reagent; Product distributionMechanism;
参考文献
Adam, Waldemar; Corma, Avelino; Martinez, Agustin; Renz, Michael
Chemische Berichte, 1996 , vol. 129, # 12 p. 1453 - 1455
反应条件
triethylamine in water; isopropyl alcohol
T=80°C; 3 h;
参考文献
Riedel
Patent: DE199148 ;