2-苯基-1,2-环氧丙烷合成路线 （共 116 条）
反应条件
1: (R)-phenylethylene oxide With sec.-butyllithium in tetrahydrofuran; hexane; cyclohexane T=-58°C; 0.000825 h; flow microreactor; 2: methyl iodide in tetrahydrofuran; hexane; cyclohexane T=-58°C; 0.000555556 h; flow microreactor;
参考文献
Chemistry - A European Journal, , vol. 16, # 47 p. 14149 - 14158
反应条件
12-molybdophosphoric acid HPMo; dihydrogen peroxide in water; acetonitrile T=50°C; 2 h;
参考文献
Journal of Materials Chemistry, , vol. 21, # 9 p. 2997 - 3005
反应条件
1: (R)-phenylethylene oxide With sec.-butyllithium in tetrahydrofuran; hexane; cyclohexane T=-38°C; 0.000861111 h; flow microreactor; 2: methyl iodide in tetrahydrofuran; hexane; cyclohexane T=-38°C; 0.000555556 h; flow microreactor;
参考文献
Chemistry - A European Journal, , vol. 16, # 47 p. 14149 - 14158
反应条件
copper diacetate in tert-butyl alcohol T=60°C; 18 h; var. solvents and metal complexes, other alkenes and adamantane, also halogenation of adamantane with CBrCl3 or t-BuOCl; Product distributionMechanism;
参考文献
Journal of the American Chemical Society, , vol. 117, # 1 p. 226 - 232
反应条件
sodium hydroxide in dichloromethane Heating;
参考文献
Tetrahedron Asymmetry, , vol. 9, # 3 p. 459 - 466
反应条件
Ni(cyclam)Br2; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide T=20°C; Carboxylation; Cyclization; Debromination; P=760 Torr; 7 h; Product distribution; Further Variations:Reagents;
参考文献
Synlett, , # 2 p. 245 - 247
反应条件
dihydrogen peroxide; polymer-anchored [VO(fsal-ea)*DMF] in acetonitrile T=80°C; Product distribution; Further Variations:TemperaturesCatalystscatalyst amount;
参考文献
European Journal of Inorganic Chemistry, , # 16 p. 2303 - 2314
反应条件
pyridine; Oxonereg;; water-d2; sodium hydrogencarbonate; pyrrolidine in acetonitrile-D3 T=20°C; 2 h; Product distribution / selectivity;
参考文献
US2003/195366 A1, ;
Page/Page column 5 ;
反应条件
tert.-butylhydroperoxide; Co3O4 in N,N-dimethyl-formamide T=69.84°C; 5 h; SonicationMolecular sieve;
参考文献
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, , vol. 52, # 6 p. 709 - 716
反应条件
sodium methylsulfinylmethanide 1.) DMSO, RT, 2 h, 2.) 3 d; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 53, # 18 p. 4190 - 4193
