反应条件
1.1: sodium tetrahydroborate; iodine / tetrahydrofuran / 18.5 h / 4 - 80 °C / Inert atmosphere 2.1: sodium carbonate / dichloromethane; water / 10.25 h / 20 °C 3.1: methanesulfonyl chloride; triethylamine / dichloromethane / 5 h / 4 - 50 °C / Inert atmosphere 4.1: copper(l) iodide; N-methyl-2-(methylamino)ethylamine / toluene / 0.33 h / 20 °C / Inert atmosphere 4.2: 21 h / 110 °C / Inert atmosphere; Sealed vessel View Scheme
参考文献
Kraut, Michael R.; Mohr, Justin T.; Stoltz, Brian M.; Schumacher, Andreas; Pfaltz, Andreas
Organic Syntheses, 2009 , vol. 86, p. 181 - 193