2-(2-溴-乙基)-萘合成路线 （共 10 条）
反应条件
N-bromosuccinmide; triphenylphosphine in dichloromethane
参考文献
Delorme, Daniel; Woo, Soon Hyung; Vaisburg, Arkadii
Patent: US2002/115826 A1, 2002 ;
反应条件
pyridine; phosphorus tribromide in benzene 6 h; Ambient temperature;
参考文献
Novak, Lajos; Rohaly, Janos; Poppe, Laszlo; Hornyanszky, Gabor; Kolonits, Pal; et al.
Liebigs Annalen der Chemie, 1992 , # 2 p. 145 - 158
反应条件
phosphorus tribromide in dichloromethane Inert atmosphere;
参考文献
MacHan, Charles W.; Spokoyny, Alexander M.; Jones, Matthew R.; Sarjeant, Amy A.; Stern, Charlotte L.; Mirkin, Chad A.
Journal of the American Chemical Society, 2011 , vol. 133, # 9 p. 3023 - 3033
反应条件
1: LiAlH4 / diethyl ether 2: PBr3 / CCl4 View Scheme
参考文献
Nishizawa, Seiichi; Cui, Ying-Yu; Minagawa, Masakazu; Morita, Kotaro; Kato, Yuichi; Taniguchi, Shinichiro; Kato, Ryo; Teramae, Norio
Journal of the Chemical Society. Perkin Transactions 2, 2002 , # 5 p. 866 - 870
参考文献
G. D. Searle and Co.
Patent: US4644071 A1, 1987 ;
US 4644071 A
反应条件
1: diethyl ether / -15 °C 2: benzene; PBr3 View Scheme
参考文献
Cagniant,P. et al.
Bulletin de la Societe Chimique de France, 1961 , p. 1934 - 1937
反应条件
1: 98 percent / LiAlH4 / diethyl ether / 2 h / 0 °C 2: 83 percent / pyridine, PBr3 / benzene / 6 h / Ambient temperature View Scheme
参考文献
Novak, Lajos; Rohaly, Janos; Poppe, Laszlo; Hornyanszky, Gabor; Kolonits, Pal; et al.
Liebigs Annalen der Chemie, 1992 , # 2 p. 145 - 158
反应条件
1-n-butyl-3-methylimidazolim hexafluoroantimonate; potassium carbonate in acetonitrile T=115°C; 58 h;
参考文献
Organic Letters, , vol. 7, # 7 p. 1231 - 1234
反应条件
water in 1,4-dioxane T=110°C; 72 h;
参考文献
Kim, Dong Wook; Hong, Dong Jin; Seo, Jai Woong; Kim, Hoon Sik; Kim, Hong Kon; Song, Choong Eui; Chi, Dae Yoon
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 3186 - 3189
反应条件
1.1: n-BuLi; NaH / tetrahydrofuran; hexane / 0.33 h / 0 °C 1.2: tetrahydrofuran; hexane / 2 h 2.1: 72 percent / ceric ammonium nitrate / acetonitrile / 4 h / 20 °C View Scheme
参考文献
Zhang, Yang; Jiao, Jingliang; Flowers II, Robert A.
Journal of Organic Chemistry, 2006 , vol. 71, # 12 p. 4516 - 4520
