Boc-L-酪氨酸羟基琥珀酰亚胺酯合成路线 （共 5 条）
反应条件
pyridine in acetonitrile T=20°C; 1.5 h; further solvent, base;
参考文献
Il'ina, A. V.; Davidovich, Yu. A.; Rogozhin, S. V.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1067 - 1070
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 5 p. 1163 - 1165
反应条件
4-methyl-morpholine in tetrahydrofuran; acetonitrile Ambient temperature;
参考文献
Jaoudai, Mahmoud; Martinez, Jean; Castro, Bertrand
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2364 - 2367
反应条件
N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide in 1,4-dioxane T=23°C; 2 h;
参考文献
Nicolaou; Hughes, Robert; Pfefferkorn, Jeffrey A.; Barluenga, Sofia; Roecker
Chemistry - A European Journal, 2001 , vol. 7, # 19 p. 4280 - 4295
反应条件
1: aq. NaHCO3 / tetrahydrofuran / 12 h / 23 °C 2: 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide / dioxane / 2 h / 23 °C View Scheme
参考文献
Nicolaou; Hughes, Robert; Pfefferkorn, Jeffrey A.; Barluenga, Sofia; Roecker
Chemistry - A European Journal, 2001 , vol. 7, # 19 p. 4280 - 4295
反应条件
1: aq. NaHCO3 / tetrahydrofuran / 12 h / 23 °C 2: 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide / dioxane / 2 h / 23 °C View Scheme
参考文献
Nicolaou; Hughes, Robert; Pfefferkorn, Jeffrey A.; Barluenga, Sofia; Roecker
Chemistry - A European Journal, 2001 , vol. 7, # 19 p. 4280 - 4295
