堪非醇 3,4'-二-O-甲醚合成路线 (共 8 条)
反应条件
1: With triethylamine Allan-Robinson condensation; 0.0833333 h; Heating; 2: With potassium hydroxide in methanol 0.333333 h; sonication;
参考文献
Daskiewicz, Jean-Baptiste; Depeint, Flore; Viornery, Lionel; Bayet, Christine; Comte-Sarrazin, Geraldine; Comte, Gilles; Gee, Jennifer M.; Johnson, Ian T.; Ndjoko, Karine; Hostettmann, Kurt; Barron, Denis
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2790 - 2804
反应条件
1.1: 65 percent / methanesulfonyl chloride; Et3N / tetrahydrofuran / 1 h / 0 °C 2.1: Et3N / 0.08 h / Heating 2.2: 81 percent / KOH / methanol / 0.33 h / sonication View Scheme
参考文献
Robinson; Shinoda
Journal of the Chemical Society, 1925 , vol. 127, p. 1977
参考文献
Lynch et al.
Journal of the Chemical Society, 1952 , p. 2063,2067
反应条件
2: pyridine; potassium carbonate View Scheme
参考文献
Lynch et al.
Journal of the Chemical Society, 1952 , p. 2063,2067
反应条件
aluminium trichloride; nitrobenzene
参考文献
Rao; Seshadri
Journal of the Chemical Society, 1947 , p. 122
参考文献
Gupta; Dhiman
Pharmazie, 1985 , vol. 40, # 5 p. 365 - 365
参考文献
Jain; Seshadri
Proceedings - Indian Academy of Sciences, Section A, 1954 , # 40 p. 249,254
参考文献
Zemplen; Bognar
Chemische Berichte, 1941 , vol. 74, p. 1783,1786