3-(噻吩-2基)丙烯酸甲酯合成路线 （共 6 条）
反应条件
triethylamine in N,N-dimethyl-formamide T=100°C; Heck reaction; P=4137.29 Torr; 0.5 h; Microwave irradiation;
参考文献
Polshettiwar, Vivek; Nadagouda, Mallikarjuna N.; Varma, Rajender S.
Chemical Communications, 2008 , # 47 p. 6318 - 6320
反应条件
potassium carbonate; triphenylphosphine in methanol T=150°C; Wittig reaction; 0.0833333 h;
参考文献
Westman, Jacob
Organic Letters, 2001 , vol. 3, # 23 p. 3745 - 3747
反应条件
palladium diacetate; triethylamine; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in N,N-dimethyl-formamide T=120°C; Heck reaction; 24 h; regioselective reaction;
参考文献
Toguem, Serge-Mitherand Tengho; Hussain, Munawar; Malik, Imran; Villinger, Alexander; Langer, Peter
Tetrahedron Letters, 2009 , vol. 50, # 35 p. 4962 - 4964
反应条件
in water T=20°C; Wittig reaction; 1 h;
参考文献
Dambacher, Jesse; Zhao, Wen; El-Batta, Amer; Anness, Robert; Jiang, Changchun; Bergdahl, Mikael
Tetrahedron Letters, 2005 , vol. 46, # 26 p. 4473 - 4477
反应条件
tri[2-(2-methoxyethoxy)ethyl]amine; potassium hexamethylsilazane in tetrahydrofuran; toluene T=-78°C; Horner-Wadsworth-Emmons reaction; 4 h;
参考文献
Tetrahedron Letters, , vol. 45, # 28 p. 5519 - 5523
反应条件
in N,N-dimethyl-formamide T=75°C; 4 h;
参考文献
Chemistry - A European Journal, , vol. 20, # 12 p. 3520 - 3527
