3-(2-羟基苯基)-丙烯酸甲酯合成路线 （共 14 条）
反应条件
in dichloromethane T=20°C; Inert atmosphere;
参考文献
Zhu, Jian-Bo; Wang, Peng; Liao, Saihu; Tang, Yong
Organic Letters, 2013 , vol. 15, # 12 p. 3054 - 3057
反应条件
chloro-trimethyl-silane T=0 - 20°C;
参考文献
Yang, Ziyin; Endo, Sakura; Tanida, Aya; Kai, Kenji; Watanabe, Naoharu
Journal of Agricultural and Food Chemistry, 2009 , vol. 57, # 14 p. 6396 - 6401
反应条件
palladium diacetate; triethylamine in acetonitrile T=70°C; Heck conditions; 40 h; Inert atmosphere;
参考文献
Fernandes, Talita De A.; Gontijo Vaz, Boniek; Eberlin, Marcos N.; Da Silva, Alcides J. M.; Costa, Paulo R. R.
Journal of Organic Chemistry, 2010 , vol. 75, # 21 p. 7085 - 7091
反应条件
1: 71 percent / bromine / CH2Cl2 / 0 °C 2: 52 percent / 1,5-diazabicyclo<4.3.0.>non-5-ene (DBN) / diethyl ether / 2 h 3: CF3COOH / H2O; tetrahydrofuran / var. pH; (2)H labelled comp. View Scheme
参考文献
Chao, Herbert S.-I.; Berchtold, Glenn A.
Journal of Organic Chemistry, 1981 , vol. 46, # 6 p. 1191 - 1194
反应条件
1: 52 percent / 1,5-diazabicyclo<4.3.0.>non-5-ene (DBN) / diethyl ether / 2 h 2: CF3COOH / H2O; tetrahydrofuran / var. pH; (2)H labelled comp. View Scheme
参考文献
Chao, Herbert S.-I.; Berchtold, Glenn A.
Journal of Organic Chemistry, 1981 , vol. 46, # 6 p. 1191 - 1194
反应条件
1: 1.) NaH / 1.) 1,2-dimethoxy ethane, room temp., 1h, 2.) reflux 0.5h 2: 71 percent / bromine / CH2Cl2 / 0 °C 3: 52 percent / 1,5-diazabicyclo<4.3.0.>non-5-ene (DBN) / diethyl ether / 2 h 4: CF3COOH / H2O; tetrahydrofuran / var. pH; (2)H labelled comp. View Scheme
参考文献
Chao, Herbert S.-I.; Berchtold, Glenn A.
Journal of Organic Chemistry, 1981 , vol. 46, # 6 p. 1191 - 1194
反应条件
tetrabutyl-ammonium chloride; triethylamine; palladium diacetate in N,N-dimethyl-formamide T=80°C; 16 h; Title compound not separated from byproducts;
参考文献
Szlosek-Pinaud, Magali; Diaz, Philippe; Martinez, Jean; Lamaty, Frederic
Tetrahedron, 2007 , vol. 63, # 16 p. 3340 - 3349
反应条件
dilithium tetrachloropalladate
参考文献
Heck,R.F.
Journal of the American Chemical Society, 1968 , vol. 90, p. 5518 - 5526
反应条件
in methanol T=60°C; Esterification; 1 h;
参考文献
Daayf, Fouad; Ongena, Marc; Boulanger, Renald; El Hadrami, Ismail; Belanger, Richard R.
Journal of Chemical Ecology, 2000 , vol. 26, # 7 p. 1579 - 1593
反应条件
caesium carbonate in toluene 27 h; Heating;
参考文献
Carlsen, Per H.J.; Liberkova, Katerina; Harrex, Rachel; Roe, Johan
Acta Chemica Scandinavica, 1997 , vol. 51, # 3 p. 343 - 344
